18-20 June, 2003, Budapest, Hungary OSSKI Center (Törley Palace)


with Exhibition and Pre-Session on Thermal Energy in Hungarian
"THERMO-BRIDGE"
between East and West for technology transfer and information exchange



Scientific Society of Measurement, Automation and Informatics (MATE)
Branch of Thermal Engineering and Thermogrammetry (TE and TGM)

Méréstechnikai, Automatizálási és Informatikai Tudományos Egyesület
Hőtechnikai és Termogrammetriai (HT és TGM) Szakosztály

MATE Secretariat: H-1372 Budapest, POB. 451.,Hungary

House of Technology, Budapest V.,Kossuth Lajos tér 6-8.III.318.
Phone: +361-332-9571, Fax:+361-353-1406
E-mail:
mate@mtesz.hu  benko@energia.bme.hu

Thermomechanics and defectometry / Hőmechanika és hibafeltárás

35/5 Early detection of corrosion damage under coatings with thermographic methods
G. Riegert1), G. Kunz2), R. Nothhelfer-Richter2) and G. Busse1)
1) Institute of Polymer Testing and Polymer Science (IKP), Department of Non-Destructive Testing (ZfP), University of Stuttgart, Pfaffenwaldring 32, D-70569 Stuttgart, Germany
2) Forschungsinstitut für Pigmente und Lacke e.V. (FPL), Allmandring 37, D-70569 Stuttgart, Germany
S5TM07
 
SUMMARY

Corrosion resistance of lacquered coated metals are tested by outdoor exposure under various climatic conditions and evaluated with standardized methods. Because of the long duration of these tests the demand for time-savinglapse tests raised. In such tests the corrosion process is accelerated by increasing the load on the sample, i.e. salt spray testing. Unfortunately the results of outdoor exposure and quick testing are not well correlated due to differences in transport and reaction mechanisms. Another approach for obtaining realistic testing results at reduced measurement duration is to improve the evaluation methods. With the early detection of corrosion damage by Pulsed Phase Thermography (PPT) the duration of outdoor exposure testing can be reduced significantly. A possible application for this kind of thermographic testing is the quality control of repaired coatings spots of lacquer. This is specially interesting for car repairs where the optical quality of the top lacquer coat layer does not show the quality of the repair itself, like hidden corrosion on the sheet metal or variation in coating layerlacquer thickness.

Pulsed Phase Thermography (PPT) uses a short light flash for sample excitation [1]. This method is the link between Pulsed Thermography (PT) [2,3] and Optical Lockin Thermography (OLT) [4,5,6]. The temperature field on the surface of the inspected object launches a thermal wave into the coatinglacquer. At hidden thermal boundaries (e.g. delaminations, corrosion) the thermal wave is reflected back to the surface of the object where it is detected. Fourier transformation of the signal provides information about the temperature amplitude and the depth of the hidden boundary layers. As a flash corresponds to a rectangular pulse it includes all a frequencies frequency spectrum for lock-in examination. The benefits of PPT isare clearly curtateda short measurement duration,with a low thermal load on the sample, and the possibility of analyzing at different frequencies andwith that hence with different depth ranges [7]. It is also possible to measure thelacquer thickness ot the layers of the coating after calibration [8]. The schematical experimental set-up is shown in figure 1.

In this paper results are presented that were obtained on model samples with different measurement und testing methods. Corrosion spots down to 0.5 mm2 under coatinglacquer layers of approx. 60 µm can be detected with the PPT method. Outdoor exposedure samples are compared to results of different short tests with corresponding duration length. With PPT it is possible to detect corrosion in an early state and thuswith that to reduce the duration of outdoor exposure tests. Another advantage of PPT as compared to conventional evaluation techniques is its non destructive (and also non-contact) character. ThereforeWith that it is possible to continue the outdoor exposure testing after evaluation in order to investigate the corrosion progress.

In addition, PPT investigations were performed on automotive parts with lacquer partly repaireds coatings.

Figure 1: Schematical sSet-up of Pulsed Phase Thermography (PPT)

References

[1] Maldague, X.; Marinetti, S.: “Pulse phase infrared thermography” Journal of Applied Physics, 79[Mar.]: 2694-2698, 1996
[2] Reynolds, W.N.: “Quality control of composite materials by thermography”, Metals and Materials, 1[2]: 100-102, 1985
[3] Cielo, P.; Maldague, X.; Déom, A.A.; Lewak, R.: “Thermographic nondestructive evaluation of industrial materials and structures”, Materials Evaluation, 45[6]: 452-460, 1987
[4] Beaudoin, J.L., Merienne, E., Danjoux, R., Egee, M.: “Numerical system for infrared scanners and application to the subsurface control of materials by photothermal radiometry”. In: Infrared Technology and Applications, SPIE Vol. 590, p. 287, 1985
[5] Kuo, P.K., Feng, Z.J., Ahmed, T., Favro, L.D., Thomas, R.L., Hartikainen, J., “Parallel thermal wave imaging using a vector lock-in video technique”. In: Photoacoustic and Photothermal Phenomena, ed. P. Hess and J. Pelzl. Heidelberg: Springer-Verlag, pp. 415-418, 1987
[6] Busse, G.: “Nondestructive evaluation of polymer materials“, NDT&E International, 27[5]:253-262, 1994
[7] Thomas, R.L., Pouch, J.J., Wong, Y.H., Favro, L.D., Kuo, P.K., Rosencwaig, A., “Subsurface flaw detection in metals by photacoustic microscopy”. In: J.Appl.Phys. Vol. 51, pp. 1152-1156, 1980
[8] Busse, G., ”Optoacoustic phase angle measurement for probing a metal”. In: Appl.Phys.Lett. Vol. 35, pp. 759-760, 1979

 

abstract

 

Contact details: Dipl.-Ing. Gernot Riegert
Institute of Polymer Testing and Polymer Science (IKP)
Department of Non-Destructive Testing (ZfP), University of Stuttgart
Pfaffenwaldring 32, D-70569 Stuttgart
Germany
Tel: +49(0)711/685-2572
Fax: +49(0)711/685-4635
Web Site:
http://www.zfp.uni-stuttgart.de
E-mail:
riegert@ikp.uni-stuttgart.de

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18-20 June, 2003, Budapest,Hungary

OSSKI Center (Törley Palace)
"Fodor József" National Center of Public Heath
"Frédéric Joliot-Curie" National Research Institute for
Radiobiology and Radiohygiene. (OKK-OSSKI)
www.osski.hu


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